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About Citrulline Citrulline Benefits Certificate of Analysis API Sourcing Citrulline Facts Contact Us

Certificate of Analysis

L-CITRULLINE
(Non-Sterile)
 
BATCH NUMBER 080101-01 MANUFACTURE DATE 2008.01.20
QUANTITY NA TEST DATE 2008.01.23
RETEST DATE 2010-01 REPORT DATE 2008.12.10
 
TEST SPECIFICATION RESULT  
Appearance White crystalline powder Conforms  
Identification HPLC Conforms  
  IR    
Specific Rotation + 24.5° ~ _ 26.8° + 25.8°  
Transmittance Note Less Than 98.0% 99.3%  
pH 5.5~7.0 (10% Water Solution) 5.9  
Heavy Metals Not More Than 10ppm <10ppm  
Ammonium Not More Than 200ppm <200ppm  
Loss on Drying Not More Than 0.30% 0.02%  
Residue on Ignition Not More Than 0.10% 0.08%  
Chloride Not More Than 200ppm <200ppm  
Sulfate Not More Than 200ppm <200ppm  
Iron Not More Than 10ppm <10ppm  
Arsenic Not More Than 1ppm <1ppm  
Assay (Calculated on dried basis) 98.5~101.0% 99.7%  
Related Substances Ornithine: Not More Than 0.5% 0.02%  
  Arginine: Not More Than 0.5% Not detected  
  Unknown Individual Impurity: Not More Than 0.1% 0.01%  
  Total Impurities: Not More Than 1.0% 0.03%  
Microbial Limits Total Count of Aerobic: Not More Than 1000 CFU/g 200CFU/g  
Fungi and Yeast: Not More Than 100 CFU/g <10CFU/g  
  Escherichia Coli: Absent/g Absent  
 
CONCLUSION: THE RESULTS CONFORM TO THE ENTERPRISE STANDARD

CITRULLINE HPLC ANALYSIS | CHEMICAL STRUCTURE